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Category 2 is the problem bucket: substances the FDA says may present significant safety risks citing issues such as immunogenicity (the body forming antibodies against an injected peptide), impurities from synthesis, and thin human data

Serum bilirubin and their association with C-reactive protein in patients with migraine

Gong W, Guo M, Han Z, Wang Y, Yang P, Xu C, et al

Mass Spectrometry (MS) Data: The COA must include mass spectrometry (MS) confirmation to verify the compounds exact molecular weight, confirming its chemical identity

doi: Antonio J, Ellerbroek A, Silver T, Vargas L, Tamayo A, Buehn R, et al