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The fourth aliquot was analyzed via negative ionization following elution from a HILIC column (Waters UPLC BEH Amide 2.1 150 mm, 1.7 m) using a gradient consisting of water and acetonitrile with 10 mM ammonium formate, pH 10.8

[DOI] [PMC free article] [PubMed] [Google Scholar] 20.Toms-Barbern F.A., Gonzlez-Sarras A., Garca-Villalba R., Nez-Snchez M.A., Selma M.V., Garca-Conesa M.T., Espn J.C